Ceramic foams are versatile materials with properties like chemical inertness, thermal shock resistance, and high-temperature stability. However, their relatively high cost of realisation has been one of the bottleneck in their wide adoption. With the advent of ceramic precursors, especially the low-cost class like siloxanes and borosiloxanes, new opportunities evolve in developing cost-effective ceramic foams from these precursors. The thesis explores some innovative methods to realize SiBOC ceramic foams with methylvinylborosiloxane as a precursor.